On crystal mosaicity in single crystal Ni-based superalloys

  • In the present work, we investigate the evolution of mosaicity during seeded Bridgman processing of technical Ni-based single crystal superalloys (SXs). For this purpose, we combine solidification experiments performed at different withdrawal rates between 45 and 720 mm/h with advanced optical microscopy and quantitative image analysis. The results obtained in the present work suggest that crystal mosaicity represents an inherent feature of SXs, which is related to elementary stochastic processes which govern dendritic solidification. In SXs, mosaicity is related to two factors: inherited mosaicity of the seed crystal and dendrite deformation. Individual SXs have unique mosaicity fingerprints. Most crystals differ in this respect, even when they were produced using identical processing conditions. Small differences in the orientation spread of the seed crystals and small stochastic orientation deviations continuously accumulate during dendritic solidification. Direct evidence for dendrite bending in a seeded Bridgman growth process is provided. It was observed that continuous or sudden bending affects the growth directions of dendrites. We provide evidence which shows that some dendrites continuously bend by 1.7° over a solidification distance of 25 mm.

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Metadaten
Author:Philipp HallenslebenGND, Felicitas ScholzGND, Pascal ThomeORCiDGND, Helge Julian SchaarGND, Ingo SteinbachORCiDGND, Gunther EggelerORCiDGND, Jan FrenzelORCiDGND
URN:urn:nbn:de:hbz:294-67440
DOI:https://doi.org/10.3390/cryst9030149
Parent Title (English):Crystals
Publisher:MDPI
Place of publication:Basel
Document Type:Article
Language:English
Date of Publication (online):2019/11/19
Date of first Publication:2019/03/13
Publishing Institution:Ruhr-Universität Bochum, Universitätsbibliothek
Tag:crystal growth; crystal mosaicity; dendrite deformation; microstructure evolution; superalloys
Volume:9
Issue:3, Artikel 149
First Page:149-1
Last Page:149-19
Institutes/Facilities:Interdisciplinary Centre for Advanced Materials Simulation (ICAMS)
Institut für Werkstoffe, Lehrstuhl Werkstoffwissenschaft
open_access (DINI-Set):open_access
faculties:Fakultät für Maschinenbau
Licence (English):License LogoCreative Commons - CC BY 4.0 - Attribution 4.0 International